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1 article(s) from Santra, Manas K

An accelerated Rauhut–Currier dimerization enabled the synthesis of (±)-incarvilleatone and anticancer studies

Tharun K. Kotammagari,
Sweta Misra,
Sayantan Paul,
Sunita Kunte,
Rajesh G. Gonnade,
Manas K. Santra and
Asish K. Bhattacharya

Beilstein J. Org. Chem. 2023, 19, 204–211, doi:10.3762/bjoc.19.19

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Figure 1: Structures of (±)-incarvilleatone (1), (±)-incarviditone (2), and (±)-rengyolone (3).

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Scheme 1: Possible modes of accelerated intermolecular RC reaction, drawn according to [6].

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Scheme 2: Retrosynthetic plan for the synthesis of (±)-incarvilleatone (1) and (±)-incarviditone (2).

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Scheme 3: Synthesis of RC dimerized product (±)-4.

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Scheme 4: Proposed reaction mechanism for the formation of compound (±)-4 under TBAF-mediated Rauhut–Currier ...

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Scheme 5: Synthesis of (±)-incarvilleatone (1) from RC dimerized product (±)-4.

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Scheme 6: Separation of rac-incarvilleatone (1) and determination of absolute configurations of both the enan...

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Scheme 7: Synthesis of (±)-incarviditone (2).

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Figure 2: Growth suppression activity of the synthesized compounds in the breast cancer cell line MCF-7.

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Published 21 Feb 2023

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